If only you wanted to convert from FAT32 to NTFS I could finally utilize all my MCSE training and all the fancy DOS TOOL commands they teach you to CONVERT /fs:ntfs..lol..ok you have to be a nerd to understand that one..sorry..
Yes as mentioned I would use Partition Magic as well to reorganize your partitions. I would try to make it as non-complicated as possible. Meaning I would concentrate first on getting the size of the partition correct THEN concentrate on making it FAT32.